Vici D-4-I-VA38-R Uživatelský manuál

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Valco Instruments Co. Inc.
Valco Instruments Co. Inc.
800
·
367
·
8424 sales
713
·
688
·
9345 tech
713
·
688
·
8106 fax
Valco International
Schenkon, Switzerland
Int + 41
·
41
·
925
·
6200 phone
Int + 41
·
41
·
925
·
6201 fax
d4_var.P65
Rev 5/12
Printed in USA
Pulsed Discharge
Detector
Model D-4-I-VA38-R
Instruction Manual
Introduction
Description and Operating Principles............................................................1
Safety Notes and Information........................................................................2
Symbols
Installation Category
Safety
Components of the Detector System............................................................3
System Requirements
Components not Included with the Detector System....................................4
System Purity................................................................................................4
Gas Specifications........................................................................................5
Installation
General Precautions......................................................................................6
Mounting the Detector on the GC.................................................................6
Gas Connections...........................................................................................7
Installing and Purging the Gas Regulator..............................................7
Installing and Purging the Helium Purifier..............................................8
Connecting the Discharge Gas to the Detector.....................................8
Capillary Column Connection........................................................................9
Packed Column Connection..........................................................................9
Testing for Leaks.........................................................................................10
Pulser Module Installation...........................................................................11
Detector Electrical Connections..................................................................12
Initial Power-Up...........................................................................................13
Troubleshooting High Background Current..................................................13
Mode Selection and Setup
Helium Ionization Mode...............................................................................14
Selective Photoionization Mode...................................................................14
Warranty............................................................................................................16
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Shrnutí obsahu

Strany 1 - Instruction Manual

Valco Instruments Co. Inc.Valco Instruments Co. Inc.800 · 367· 8424 sales713 · 688· 9345 tech713 · 688· 8106 [email protected] InternationalSchen

Strany 2

8InstallationEZR217. Open the cylinder valve to pressurize the regulator once again. Close thevalve and observe the needle of the high pressure gauge

Strany 3 - Introduction

9InstallationCapillary Column ConnectionIf the capillary column adapter is installed in the column inlet:1. Make a mark on the column 11.4 cm from the

Strany 4 - Safety Notes and Information

103. Set aside the 1/8" wrench and completely remove the adapter from thecolumn inlet.4. Screw the packed column adapter into the column inlet by

Strany 5

11InstallationPulser Module Installation1. Mount the pulser module in the pneumatics area of the GC, using existingslotted screw holes. (Figure 5)2.

Strany 6 - System Requirements

12InstallationDetector Electrical ConnectionsCAUTION: Do not use a wrench to tighten the SMCconnectors on the bias and electrometer cables.Connections

Strany 7 - Gas Specifications

13InstallationInitial Power-Up1. Set the discharge gas flow as specified in Figure 4 on page 7.CAUTION: Always make sure that discharge gas isflowing

Strany 8 - Installation

14Mode Selection and SetupHelium Ionization ModeIf the instructions of Step 1 at the top of page 9 were properly executed,the column should already be

Strany 9 - Gas Connections

15Mode Selection and SetupAr-PDPIDChanging the discharge gas from helium to a mixture of 2% argon inhelium changes the photon energy level from the 17

Strany 10

16WarrantyThis Limited Warranty gives the Buyer specific legal rights, and a Buyermay also have other rights that vary from state to state. For a peri

Strany 11 - Packed Column Connection

This page is intentionally left blank for printing purposes

Strany 12 - Testing for Leaks

1IntroductionDescription and Operating PrincipleThe PD-D-4-I-VA38-R is a non-radioactive pulsed discharge ionization detector(PDID) which is optimized

Strany 13 - Pulser Module Installation

2Helium Ionization (PDHID)The PDHID is essentially non-destructive (0.01 - 0.1% ionization) and highlysensitive. The response to organic compounds is

Strany 14

3Components of the Detector SystemComponents of the detector system are listed in the Table 1. Check thecontents of the packages to verify that every

Strany 15 - Initial Power-Up

4IntroductionSystem RequirementsComponents Not Included with the Detector System • Helium (99.999% purity) and other support gases • Ultra high puri

Strany 16 - Mode Selection and Setup

5IntroductionedoMrotceteDDIHDPDIPDP-rADIPDP-rKDIPDP-eXsagegrahcsiDmuileHeHnirA%2eHnirK%5.1eHnieX%8.0sagreirraCmuileH*****Gas Specifications** Any gas

Strany 17

6DETECTOR MOUNTING BASEHEATERCABLEMOUNTING BASESCREWS (4)HEATER BLOCKSCREWS (2)TEMPERATUREPROBEHEATER BLOCKInstallationGeneral Precautions• Do not use

Strany 18 - Warranty

7InstallationGAS CHROMATOGRAPHCROSS(ZX1)HELIUMPURIFIERDISCHARGE GAS(99.999% He)TGA-R-35F80PRESTRICTOR(35 mL/min minimum)VENTCOLUMNINLETDISCHARGE GASIN

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