Vici D-4-I-VA38-R Uživatelský manuál

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Valco Instruments Co. Inc.
Pulsed Discharge
Detector
Model D-4-I-VA38-R
Instruction Manual
Rev 1/15
Valco Instruments Co. Inc.
800 · 367· 8424 sales
713
· 688· 9345 tech
713
· 688· 8106 fax
VICI AG International
Schenkon, Switzerland
Int + 41
· 41 · 925· 6200 phone
Int + 41
· 41 · 925· 6201 fax
North America, South America, and Australia/Oceania contact: Europe, Asia, and Africa contact::
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Strany 1 - Instruction Manual

Valco Instruments Co. Inc.Pulsed Discharge Detector Model D-4-I-VA38-R Instruction Manual Rev 1/15 Valco Instruments Co. Inc.800 · 367· 8424 sales 71

Strany 2

6DETECTOR MOUNTING BASEHEATERCABLEMOUNTING BASESCREWS (4)HEATER BLOCKSCREWS (2)TEMPERATUREPROBEHEATER BLOCKInstallationGeneral Precautions• Do not use

Strany 3 - Table of Contents

7InstallationGAS CHROMATOGRAPHCROSS(ZX1)HELIUMPURIFIERDISCHARGE GAS(99.999% He)TGA-R-35F80PRESTRICTOR(35 mL/min minimum)VENTCOLUMNINLETDISCHARGE GASIN

Strany 4

8InstallationEZR217. Open the cylinder valve to pressurize the regulator once again. Close thevalve and observe the needle of the high pressure gauge

Strany 5 - Introduction

9InstallationCapillary Column ConnectionIf the capillary column adapter is installed in the column inlet:1. Make a mark on the column 11.4 cm from the

Strany 6 - Safety Notes and Information

103. Set aside the 1/8" wrench and completely remove the adapter from thecolumn inlet.4. Screw the packed column adapter into the column inlet by

Strany 7

11InstallationPulser Module Installation1. Mount the pulser module in the pneumatics area of the GC, using existingslotted screw holes. (Figure 5)2.

Strany 8 - The discharge gas

12InstallationDetector Electrical ConnectionsCAUTION: Do not use a wrench to tighten the SMCconnectors on the bias and electrometer cables.Connections

Strany 9 - Gas Specifications

13InstallationInitial Power-Up1. Set the discharge gas flow as specified in Figure 4 on page 7.CAUTION: Always make sure that discharge gas isflowing

Strany 10 - Installation

14Mode Selection and SetupHelium Ionization ModeIf the instructions of Step 1 at the top of page 9 were properly executed,the column should already be

Strany 11 - Gas Connections

15Mode Selection and SetupAr-PDPIDChanging the discharge gas from helium to a mixture of 2% argon inhelium changes the photon energy level from the 17

Strany 12

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Strany 13 - Packed Column Connection

16WarrantyThis Limited Warranty gives the Buyer specific legal rights, and a Buyermay also have other rights that vary from state to state. For a peri

Strany 14 - Exercise

Table of ContentsIntroduction Description and Operating Principles ...1 Safety Notes an

Strany 15 - Pulser Module Installation

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Strany 16

1IntroductionDescription and Operating PrincipleThe PD-D-4-I-VA38-R is a non-radioactive pulsed discharge ionization detector(PDID) which is optimized

Strany 17 - Initial Power-Up

2Helium Ionization (PDHID)The PDHID is essentially non-destructive (0.01 - 0.1% ionization) and highlysensitive. The response to organic compounds is

Strany 18 - Mode Selection and Setup

3Components of the Detector SystemComponents of the detector system are listed in the Table 1. Check the contents of the packages to verify that eve

Strany 19

4IntroductionSystem RequirementsComponents Not Included with the Detector System • Helium (99.999% purity) and other support gases • Ultra high puri

Strany 20 - Warranty

5IntroductionedoMrotceteDDIHDPDIPDP-rADIPDP-rKDIPDP-eXsagegrahcsiDmuileHeHnirA%2eHnirK%5.1eHnieX%8.0sagreirraCmuileH*****Gas Specifications** Any gas

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